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Beilstein J. Org. Chem. 2015, 11, 1991–1996, doi:10.3762/bjoc.11.215
Graphical Abstract
Figure 1: Members of the panicein family of aromatic sesquiterpenoids.
Figure 2: Proposed biogenesis of panicein A2 (5).
Figure 3: Retrosynthetic analysis of panicein A2 (5).
Scheme 1: Synthesis of ketone 13.
Scheme 2: Synthesis of propargyl ether 8 through formation of trifluoroacetate intermediate 17.
Scheme 3: Synthesis of propargyl ether 8 through carbonate 18.
Scheme 4: Synthesis of panicein A2 (5).